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We wish to report here our initial efforts toward the total synthesis of the potent antitumor agent dictyostatin, describing a short and efficient synthesis of the C11–C23 fragment. (© Wiley-VCH Verlag GmbH & Co. KGaA, 69451 Weinheim,... more
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The stereocontrolled synthesis of β-galactosyl-5-aza-sphinganines was accomplished with high efficiency by a novel and convergent strategy. The truncated β-galactosphinganine 5 was easily acylated with different long chains. Moreover, the... more
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Ion exchange reactions between the Dion-Jacobson-type, triple-layered perovskite RbCa2Nb3O10 and calcium, strontium, and barium cations were investigated. Exchange occurs in all systems, but only the strontium and barium systems form... more
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A complete set of platinum(II) solketal substituted phthalocyanines has been synthesized and characterized. To evaluate their potential as Type II photosensitizers for photodynamic therapy, comparative studies of their photophysical and... more
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The preparation of 2-triazolyl- and 2-triazolylmethylpyrrolidines from L-proline and L-trans-4-hydroxyproline is described, along with their evaluation as chiral ligands in ruthenium-catalyzed asymmetric transfer hydrogenation. Modular... more
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Some 35 years ago, I had the good fortune to be accepted into Ray Wu’s lab as a graduate student. Ray was already well known for his pioneering studies in DNA sequencing, and his lab was quietly humming with the excitement of the new... more
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Tripodal peptide analogues were designed on the basis of the phosphotyrosine binding pocket of the Src SH2 domain and assayed for their ability to bind to fluorescein-labeled phosphopeptides. Fluorescence polarization assays showed that a... more
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Xanthophylls are oxygenated carotenoids abun-dant in the human food supply. Lutein, zeaxanthin, and cryptoxanthin are major xanthophyll carotenoids in human plasma. The consumption of these xanthophylls is directly associated with... more
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In this work, TiO2 photocatalysts were synthesized using a conventional sol-gel and hydrothermal synthesis methods with steam pressure treatment. Photocatalysts were characterized by X-ray diffraction (XRD), diffuse reflectance spectra... more
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